Abstract
The crystal structure of the spinel CoNi2S4 was refined from X-ray and neutron powder-diffractometer data. The lattice parameter at room temperature and the positional parameter of the sulfur atom were determined as 9.424(1) Å and 0.2591(3). The neutron intensities show clearly that CoNi2S4 is an inverse spinel, Ni[CoNi]S4.

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