Abstract
The polarised single-crystal electronic and e.s.r. spectra of 2,2′-bipyridylbis(hexafluoroacetylacetonato)copper(II) have been measured. The correlation of the single-crystal electronic and e.s.r. spectral data with the crystallographic data indicates a dxy ground state. The polarised single-crystal electronic spectra are interpreted in D2 effective symmetry and yield a tentative one-electron orbital sequence dxy > dz2 > dyz > dxz > dx2y2. The energy of the dz2dxy transition (9·4 kk) is consistent with the restricted tetragonal distortion suggested by the crystal structure. The combined spin-orbit and orbital-reduction parameters are calculated and the values discussed in terms of π-bonding within the molecule.

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