Synthesis of a stable sulfenic acid, trans-decalin-9-sulfenic acid
- 1 January 1992
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 18,p. 1337-1338
- https://doi.org/10.1039/c39920001337
Abstract
Hydrolysis of trans-9-decalyl methoxymethyl sulfoxide with 7% perchloric acid in MeOH–H2O (2 : 1) gave crystalline trans-decalin-9-sulfenic acid whose structure was confirmed by IR, NMR and mass spectrometry; addition to methyl propiolate affording methyl trans-3-(trans-9-decalylsulfinyl)acrylate.Keywords
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