Application of microwave dielectric loss heating effects for the rapid and convenient synthesis of intercalation compounds
- 1 January 1989
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 20,p. 1515-1517
- https://doi.org/10.1039/c39890001515
Abstract
Intercalation compounds of α-VO(PO4)·2H2O with pyridine, 4-methylpyridine, and 4-phenylpyridine have been synthesised two orders of magnitude more quickly using microwave dielectric loss heating effects than with conventional thermal methods; the samples retain a high degree of crystallinity and are therefore readily characterised by powder X-ray crystallographic techniques.Keywords
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