Synthesis of (±)-2-fluorograndisol

Abstract
(±)-2-Fluorograndisol (2) was synthesised by ring expansion–fluorination from 3-(1-isopropenylcyclopropyl)butane-1,3-diol methanesulphonate (15) with a Pri 2NH–KHF2–(HF)n·Py complex (Py = pyridine).

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