High-temperature NMR using inductive heating
- 1 January 1990
- journal article
- research article
- Published by AIP Publishing in Review of Scientific Instruments
- Vol. 61 (1) , 77-80
- https://doi.org/10.1063/1.1141903
Abstract
We report a simple, efficient method for carrying out nuclear magnetic resonance(NMR) experiments at high temperature in any NMR probe without modification. The sample tube is coated with a thin film of metal and the rf coil used for the NMR experiment is used to inductively heat the film, thus heating the sample inside the tube. Using this approach, we have obtained both proton and high‐resolution carbon‐13 NMR spectra at temperatures as high as 730 K.Keywords
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