Synthesis and X-ray analysis of unusual planar tetra- and hexa-nuclear osmium clusters containing trifluoroacetate ligands

Abstract
The compounds Os6(CO)18(O2CCF3)2(1) and Os4(CO)12(O2CCF3)2(2), isolated in low yields from the reaction of Os6(CO)18 with Hg(O2CCF3)2, have been found by X-ray analysis to have unusual planar arrangements of the metal atoms.

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