Crystal and molecular structure of bisaquabis(thiobenzoato)zinc(II)
- 1 January 1976
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in J. Chem. Soc., Dalton Trans.
- No. 1,p. 67-70
- https://doi.org/10.1039/dt9760000067
Abstract
The crystal and molecular structure of the title compound has been determined from photographic X-ray data by the heavy-atom technique and refined by anisotropic least-squares methods to R 0.062 for 908 visually estimated reflections. Crystal are monoclinic, space group C2, with Z= 2, in a unit cell of dimensions: a= 9.836, b= 6.809, c= 11.915 Å, β= 108°12′ The tetrahedra zinc environment consists of two water molecules and two monothiobenzoate groups bonding as unidentate ligands through sulphur, with a shortest Zn–S distance 2.278(2)Å.Keywords
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