A Paramagnetic Diniobium Complex with a Very Short Nb−Nb Distance: Evidence for a Pseudo Nb−Nb Triple Bond?

Abstract
In spite of the short Nb−Nb distance (2.268 Å) and the presumable existence of an Nb≡Nb bond, the paddle-wheel-shaped diniobium(II) complex 1 is paramagnetic. Theoretical calculations indicate that the presence of LiCl moieties on the intermetallic axis lowers the Nb−Nb bond order and is responsible for the observed paramagnetism.

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