General and Efficient Synthesis of 1,1,1-Trichloro-2-alkanols
- 1 January 1990
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1990 (04) , 327-328
- https://doi.org/10.1055/s-1990-26866
Abstract
1,1,1-Trichloroalkanols were readily obtained in good yields by reaction of trichloroacetic acid with aldehydes in hexamethylphosphoric triamide. 1,3-Dimethyl-2-imidazolidinone was found to be useful as an alternate solvent giving, however, lower yields.Keywords
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