An Improved Method for the Synthesis of 1-lodoalkynes
- 1 January 1987
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1987 (07) , 661-662
- https://doi.org/10.1055/s-1987-28042
Abstract
A simple and general one-pot procedure for the synthesis of 1-iodoalkynes is described based on the reaction of terminal acetylenes with bis(pyridine)iodine(I) tetrafluoroborate in the presence of sodium methoxide. The method now reported is superior to the literature procedures in scope, handling, and often yield.Keywords
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