Simplified method for analyzing nanoindentation data and evaluating performance of nanoindentation instruments
- 1 November 2001
- journal article
- Published by Springer Nature in Journal of Materials Research
- Vol. 16 (11) , 3084-3096
- https://doi.org/10.1557/jmr.2001.0426
Abstract
Nanoindentation is a simple and effective means for evaluating the mechanical properties of thin films. In such circumstances, nanoindentation testers have been developed and commercialized by some companies. In this study, we tested the standard four specimens using six different types of testers and established a method to evaluate the nanoindentation data. The method requires only two correction factors; one is the frame compliance, Cf, of the testers, and the other is the error of the detection of the original surface which includes both the truncation of the indenter apex and the damage of the surface caused by the preloading of the indenter. The latter correction is conducted by adding a correction length, ΔhC, to the measured penetration depth, h. It was found that the values ΔhC increase with decrease in the hardness of material and are very sensitive to the performance of the testers.Keywords
This publication has 10 references indexed in Scilit:
- Determination of indenter tip geometry and indentation contact area for depth-sensing indentation experimentsJournal of Materials Research, 1998
- Development of a depth controlling nanoindentation tester with subnanometer depth and submicro-newton load resolutionsReview of Scientific Instruments, 1997
- An alternative method for penetration depth determination in nanoindentation measurementsJournal of Materials Research, 1997
- Nanoindentation of glass with a tip-truncated Berkovich indenterPhilosophical Magazine A, 1996
- Elastic analysis of triangular pyramidal indentation by the finite-element method and its application to nano-indentation measurement of glassesPhilosophical Magazine A, 1994
- An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experimentsJournal of Materials Research, 1992
- A Scanning Electron Microscope With Two Secondary Electron Detectors and Its Application to the Surface Topography Measurements of Magnetic MediaJournal of Tribology, 1992
- Elastic analysis of some punch problems for a layered mediumInternational Journal of Solids and Structures, 1987
- A method for interpreting the data from depth-sensing indentation instrumentsJournal of Materials Research, 1986
- The relation between load and penetration in the axisymmetric boussinesq problem for a punch of arbitrary profileInternational Journal of Engineering Science, 1965