The Electrodeposition of Molybdenum from Aqueous Solutions

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Abstract
A survey of the literature shows that G. F. Yntema claims that molybdenum can be deposited from an aqueous bath. The authors were unable to obtain bright deposits by following the method he outlined. In the experimental work of the authors, conditions were found for the plating of smooth, adherent, steel gray deposits of molybdenum, from an aqueous solution prepared by the electrolytic reduction of molybdic acid anhydride dissolved in sulfuric acid, using platinum electrodes. Baths were prepared both electrolytically and chemically and were used with and without addition agents. An attempt was made to obtain metallic deposits from each bath. Steel gray deposits of molybdenum were obtained under carefully controlled conditions.

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