Determination of Alpha-Tocopherol Levels in Rat Microsomes by High-Performance Liquid Chromatography

Abstract
A rapid, simple and sensitive method is described for the routine determination of alphatocopherol in microsomes. After a single extraction step with n-heptane extracts are injected onto a normal phase column using n-heptane/isopropanol (99.3/0.7, v/v) for elution; a fluorescence detector set at 215 nm excitation wavelenght and a cut-off filter emitting at 320 nm are used for detection. Total run time is less than 4 minutes.

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