Cyclic n-Butylboronates as Derivatives of Polar Bifunctional Groups for Gas Chromatography and Mass Spectrometry

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Abstract
An analytical study has been made of the reaction of n-butylboronic acid with a variety of polar bifunctional compounds. 1,2- and 1,3-Diols, α- and β-hydroxyacids, and 1,2- and 1,3-hydroxyamines were rapidly converted to cyclic boronate derivatives, which showed satisfactory gas chromatographic behaviour. Characteristic features of the mass spectra are reported.

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