Structure of (KSO3)2NO in X-Irradiated Single Crystals of (KSO3)2NOH

Abstract
The nitrosyldisulfonate ion has been identified in x-irradiated single crystals of potassium hydroxylaminedisulfonate. Principal values of the N14 hyperfine coupling constants are 27.5, 7.7, and 5.5 G. The principal g values are 2.0094, 2.0055, and 2.0026. Weak transitions due to hyperfine interactions with a proton from the host crystal are observed.