Analysis of classes of compounds of environmental concern: III. Organochlorine pesticides

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Abstract
Forty five organochlorine pesticides (currently listed in EPA Method 8081A) have been chromatographed on DB‐5/DB‐1701 and SPB‐5/SPB‐1701 column pairs which were in each case connected to an inlet splitter and separate electron capture detectors. Thirteen additional compounds were evaluated for their suitability as internal standards or surrogate compounds for incorporation into Method 8081A. Method reproducibility and linearity are discussed, and results are presented for extracts of six real samples spiked with fifteen organochlorine pesticides and analyzed using the dual‐column, dual‐detector arrangement.

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