Liquid Chromatographic Determination of Azide as the 3,5-Dinitrobenzoyl Derivative
- 1 January 1982
- journal article
- research article
- Published by Taylor & Francis in Journal of Liquid Chromatography
- Vol. 5 (4) , 597-604
- https://doi.org/10.1080/01483918208060571
Abstract
A method for the determination of azide after conversion to 3,5-dinitrobenzoyl azide has been developed. The derivatization reaction is fast (3 min.), quantitative, and yields a product with strong ultraviolet absorption. The derivatization reaction mixture is separated by high performance liquid chromatography so that the azide derivative can be easily quantitated. The detection limit of the method is 10 ng NaN3/mL. The total analysis time is 20 minutes per sample.This publication has 3 references indexed in Scilit:
- Microdetermination of chloride and azide by sequential titrationMicrochimica Acta, 1971
- Determination of Azide Ion by Hydrogen Ion Titration after Oxidation with Nitrite.Analytical Chemistry, 1965
- Determination of Hydrazoic Acid and Ferric Ion by Spectrophotometric Measurement of the Ferric Azide ComplexAnalytical Chemistry, 1961