Röntgenaufnahmen mit der Buergerschen Präzessionskamera bei Temperaturen zwischen 1000°C und 2000°C

Abstract
Single crystal photographs at temperatures between 1000°C and 2000°C using a Buerger precession camera can be obtained by heating the crystal with a small gas flame. The temperature of exposure may be controlled by gas pressure and gas flow (pressure regulator and needle valve). Advantages and disadvantages of the device are discussed. X-ray exposures at high temperatures of anorthite (CaAl 2 Si 2 O 8 ) demonstrate the application of the apparatus. The lattice angle α * and the intensity ratios of some reflections show a continuous change at temperatures between 300°C and 1400°C.

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