RADIOENZYMATIC MICROMETHOD FOR THE DETERMINATION OF UDP-GLUCURONIC ACID

  • 1 January 1979
    • journal article
    • research article
    • Vol. 17  (6) , 363-367
Abstract
A new sensitive and specific micromethod for determination of UDP-glucuronic acid is described. Extracts from 2.5 mg of liver are incubated with twice-washed guinea pig microsomes (as a source of UDP-glucuronyl transferase) and [14C]p-nitrophenol. The content of UDP-glucuronic acid is calculated from the [14C]p-nitrophenyl glucuronide/[14C]p-nitrophenol radioactivity ratio and the known amount of introduced [14C]p-nitrophenol. These values are corrected for losses of UDP-glucuronic acid by a calibration experiment, containing a known amount of UDP-glucuronic acid. Mean concentration of UDP-glucuronic acid in mice liver was 171 .mu.mol/kg wet weight.