Peptide sweeteners. 6. Structural studies on the C-terminal amino acid of L-aspartyl dipeptide sweeteners

Abstract
Stereochemical and structural aspects of the variations in the C-terminal residue of L-aspartyl-L-phenylalanine methyl ester were investigated. Novel configurational analogs such as L-aspartyl-D-alanine benzyl ester and L-aspartyl-D-.alpha.-aminobutyric acid benzyl ester were sweet. Chiral and achiral .alpha.,.alpha.-dialkylglycine and .alpha.-aminocycloakanecarboxylic acid were incorporated into the dipeptides. The L-aspartic acid based dipeptide derivatives of .alpha.-aminoisobutyric acid methyl ester, .alpha.-aminocyclopropanecarboxylic acid methyl ester, .alpha.-aminocyclobutanecarboxylic acid methyl ester and .alpha.-aminocyclopentanecarboxylic acid methyl ester were sweet. Dipeptides with .apprx.-aminocyclohexanecarboxylic acid methyl ester and .alpha.-aminocycloheptanecarboxylic acid methyl ester were bitter, whereas the analog with .alpha.-aminocylooctanecarboxylic acid methyl ester, .alpha.,.alpha.-diethylglycine methyl ester and .alpha.-aminoisobutyric acid benzyl ester were tasteless. Aspects on chirality and effective volume of the C-terminal residue are discussed and correlated with taste.

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