A Proton NMR Study of Ribosomal Protein L25 from Escherichia coli

Abstract
A highly folded form of the ribosomal protein L25 from E. coli can be obtained from unrea-denatured preparations. Proton NMR data show that this form of the molecule must have a compact, globular tertiary structure. Spectroscopically it is indistinguishable from L25 prepared by methods which avoid denaturing solvents. Thus L25 is a protein which can be reversibly denatured. The stability and solubility of the folded form of the protein are discussed and primary assignments made for a number of resonances in its NMR spectrum. This folded form of the protein can be characterized using NMR spectroscopy. High-resolution NMR spectroscopy provides a sensitive and general way for the characterization of protein folds.