Crystal Structure of 4‐Trimethyltin‐quinuclidinium Perchlorate
- 23 April 1980
- journal article
- research article
- Published by Wiley in Helvetica Chimica Acta
- Vol. 63 (3) , 750-753
- https://doi.org/10.1002/hlca.19800630326
Abstract
The crystal structure of 4‐trimethyltin‐quinuclidinium perchlorate has been determined by direct methods and refined by least squares techniques. Crystals of C10H22ClNO4Sn are monoclinic, space group I2/c with lattice parameters a = 29.445 (13), b = 18.400(8), c = 11.300(5) Å, β = 95.82(5)°, V = 6090.65Å3, and two independent molecules (Z = 16), Interatomic distances are compared with those of known structures of quinuclidinium chloride and 4‐haloquinuclidinium chlorides and perchlorates.Keywords
This publication has 4 references indexed in Scilit:
- A Reexamination of Inductive Substituent Constants Derived from pKa Values of 4-Substituted Quinuclidines. Polar effects. Part VIIIHelvetica Chimica Acta, 1980
- Relativistic Calculation of Anomalous Scattering Factors for X RaysThe Journal of Chemical Physics, 1970
- X-ray scattering factors computed from numerical Hartree–Fock wave functionsActa Crystallographica Section A, 1968
- Coherent X-Ray Scattering for the Hydrogen Atom in the Hydrogen MoleculeThe Journal of Chemical Physics, 1965