Assignment of the carbon-13 spectrum of vancomycin and its derivatives
- 1 January 1981
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 2
- No. 1,p. 201-206
- https://doi.org/10.1039/p29810000201
Abstract
The antibiotic vancomycin and its derivatives CDP-I and aglucovancomycin have been studied by 13C n.m.r. spectroscopy. The spectra have been partially assigned by means of model compounds, pH titrations, addition of lanthanide ions, selective {1H} decoupling, and 13C labelling experiments, allowing all but four of the 66 carbon atoms in vancomycin to be assigned. Full details of the assignment are presented.Keywords
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