The spatial resolution of X-ray microanalysis in the scanning transmission electron microscope
- 1 May 1980
- journal article
- research article
- Published by Taylor & Francis in Philosophical Magazine A
- Vol. 41 (5) , 761-775
- https://doi.org/10.1080/01418618008239347
Abstract
The spatial resolution of X-ray microanalysis within thin foils in the scanning transmission electron microscope (STEM), interfaced with an energy dispersive X-ray spectrometer, has been analysed. The electron beam divergence within the foil has been described analytically and the resulting X-ray intensity profiles have been numerically evaluated for a range of simple elemental composition distributions within the foil. The effects of incident electron probe diameter, electron accelerating voltage and foil thickness on the measured X-ray intensity ratio profiles are considered and discussed.Keywords
This publication has 11 references indexed in Scilit:
- A comparison of X-ray (STEM) and Auger electron spectroscopy for the microanalysis of grain boundary segregationPhilosophical Magazine A, 1978
- Microanalysis of Grain Boundary Segregation in Embrittled Iron‐3wt% Nickel Alloys Using STEMJournal of Microscopy, 1978
- Limitations in the X-ray microanalysis of thin foils in a scanning transmission electron microscopeJournal of Microscopy, 1977
- Improved spatial resolution microanalysis in a scanning transmission electron microscopeX-Ray Spectrometry, 1977
- Segregation and the strength of grain boundariesProceedings of the Royal Society of London. Series A. Mathematical and Physical Sciences, 1976
- Equilibrium segregation in a ternary solution: A model for temper embrittlementSurface Science, 1975
- Electron Beam MicroanalysisPublished by ASTM International ,1972
- Electron-probe microanalysis: Instrumental and experimental aspectsInternational Materials Reviews, 1969
- The angular distribution of characteristic x radiation and its origin within a solid targetProceedings of the Physical Society, 1964
- Multiple Scattering in an Infinite MediumPhysical Review B, 1950