Abstract
New mixed-valence-compounds with Sb(III) and Sb(V) of the structure (RH+)8(Cl-)4SbCl6 3-SbCl6 - with R equal CH3CH(NH2)CH3, CH3CH(NH2)CH2CH3, CH3CH2CH2NH2, and CH3CH(CH2NH2)CH3 are reported. Different methods of preparation for these compounds are described. Compounds with the structure (RH+)8(Br-)4SbCl6 3-SbCl6 - are obtained with R = CH3CH(NH2)CH2CH3 and CH3CH(NH2)CH3. All compounds are characterised, their formation is discussed

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