Determination of Trace Elements in Serum Using Inductively Coupled Plasma Atomic Spectroscopy with Hydride Generation and Chelating Resin Preconcentration
- 1 September 1984
- journal article
- Published by SAGE Publications in Applied Spectroscopy
- Vol. 38 (5) , 635-644
- https://doi.org/10.1366/0003702844554855
Abstract
A procedure is described for the inductively coupled plasma emission spectroscopic determination of Cd, Co, Cu, Fe, Mo, V, and Zn in < 1 mL of serum after digestion in nitric and perchloric acids and preconcentration with a poly(dithiocarbamate) resin Recoveries are 91 to 106% The determination of As and Se in serum by hydride generation and ICP-AES is performed after the interference of Cu on Se hydride generation was reduced by complexation of the Cu with poly(acrylamidoxime) resin Verification with NBS-SRMs as well as with human sera samples is reportedKeywords
This publication has 47 references indexed in Scilit:
- A critical comparative study of atomic-spectrometric methods (atomic absorption, atomic emission and inductively coupled plasma emission) for the determination of strontium in biological materialsThe Analyst, 1983
- Trace element analysis of biological materials by thermal and epithermal neutron activation analysisJournal of Radioanalytical and Nuclear Chemistry, 1981
- Normal levels of trace elements in human blood plasma or serumAnalytica Chimica Acta, 1980
- Determination of cobalt in bloodThe Analyst, 1980
- Communications. Determination of cadmium in blood after destruction of organic material by low-temperature ashingThe Analyst, 1980
- Determination of silicon and aluminum in biological matrixes by inductively coupled plasma emission spectrometryAnalytical Chemistry, 1980
- Dosage du baryum dans l'eau et les liquides biologiques par spectrometrie d'emission avec source plasma haute frequenceAnalytica Chimica Acta, 1979
- Determination of aluminum in blood, urine, and water by inductively coupled plasma emission spectrometryAnalytical Chemistry, 1979
- Comparison of three analytical methods for the determination of trace elements in whole bloodAnalytica Chimica Acta, 1979
- The determination of trace metals in microlitre samples by plasma torch excitationAnalytica Chimica Acta, 1972