Hydrogen bonding ino-aminophenol hydrochloride
- 1 November 1965
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Kristallographie
- Vol. 122 (3) , 283-297
- https://doi.org/10.1524/zkri.1965.122.3-4.283
Abstract
The crystal data are: a = 10.280 Å, b = 4.938 Å, c = 28.010 Å, β = 98.12°, Dm = 1.37 g · cm−3, Z = 8, Dx = 1.36 g · cm−3. Space group P21/c. The structure, which has been solved by conventional methods and refined by least squares, has two molecules per asymmetric unit. Each Cl− ion participates in four hydrogen bonds: the first contacts two O atoms (3.01 and 3.07 Å) and two N atoms (3.18 and 3.19 Å) whilst the second contacts four N atoms (3.13, 3.17, 3.20 and 3.24 Å). The angles are roughly tetrahedral. All eight bonding hydrogen atoms have been detected in a difference map.Keywords
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