Synthese von α-Halogen-ω-alkylthio-alkanen und α,ω-Bisalkylthio-alkanen
- 1 January 1987
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1987 (09) , 841-843
- https://doi.org/10.1055/s-1987-28097
Abstract
Synthesis of α-Halogeno-ω-alkylthioalkanes and α,ω-Bisalkylthioalkanes The reaction of α,ω-dihalogenated alkanes [X(CH2)nX,,n = 3 - 10]with alkylthiolates affords α-halogeno-ω-alkylthioalkanes 1 as well as α,ω-bisalkylthioalkanes 2. Products 1 (40 examples) and 2 (22 examples) are easily isolated in good yields by flash chromatography.Keywords
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