Application of triple-channel 13C{1H,19F} NMR techniques to probe structural properties of disordered solids
- 1 January 1997
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 21,p. 2045-2046
- https://doi.org/10.1039/a705053d
Abstract
Triple-channel 13C MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach involving a combination of 1H→13C and 19F→13C cross-polarization experiments, with both single-channel (1H) and double-channel (1H,19F) decoupling is developed to assign resonances for a given type of 13C nucleus in different intermolecular environments.Keywords
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