Abstract
Reaction of trans-bromotetracarbonyl(phenylcarbyne)-complexes of chromium, molybdenum and tungsten and trans-bromotetracarbonyl(methylcarbyne) complexes of chromium and tungsten with the bidentate ligands 2,2′-bipyridyl and 1,10-phenanthroline results in the replacement of two carbonyl groups leading to very thermostable carbyne complexes with the general formula Br(CO)2LMCR (L: 2,2′-bipy, ophen; M: Cr, Mo, W; R : CH3, C6H5).

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