Flow Electrosyntheses of Group II–VI Compound Semiconductor Thin Films and Composition‐modulated Superstructures

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Abstract
Stoichiometric and thin films and alternating (nanomodulated) layers of and were electrosynthesized on polycrystalline Ti substrates using a flow technique. A potential step‐hold sequence was employed coupled with solution flow (5 ml/min) wherein was used to generate , and was the starting medium composition for . For the electrosynthesis of … superstructures, these two bath composition modulations were interspersed with a 1M “wash” step.

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