Co-ordinating properties in aqueous solution of the oxygen atom in bis-2-aminoethyl ether

Abstract
The stability constants of the NiII, CuII, and ZnII complexes with bis-2-aminoethyl ether (oden) have been determined at 25 °C in 0·5M-KNO3 and the enthalpies of reaction determined calorimetrically under the same conditions. The results are compared with those for diethylenetriamine (den). In all the complexes investigated the co-ordination of the oxygen atom is achieved. The simple MII(oden) complexes are less stable than the corresponding den complexes, and the determining factor in the destabilisation is a less favourable enthalpic contribution. Thus we might consider the co-ordination of the ether oxygen atom as an endothermic process. The results obtained for the hydroxo-species [Cu(OH)(oden)]+ and [Zn(OH)(oden)]+ are different from results previously obtained for similar species. Explanations are suggested.

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