Novel conformation and synthesis of octakis(cyclohexylthio)naphthalene

Abstract
The crystalline title compound 1, prepared from both perfluoronaphthalene and, in a remarkable new reaction, perfluorodecalin 3 has been shown by X-ray and solid-state NMR spectroscopic methods to have an axial C-S bond in one of the four crystallographically independent cyclohexane rings.

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