Crystallite size determination of nylon 6 by wallner's method
- 1 July 1974
- journal article
- research article
- Published by Wiley in Journal of Polymer Science: Polymer Physics Edition
- Vol. 12 (7) , 1491-1497
- https://doi.org/10.1002/pol.1974.180120721
Abstract
The crystallite sizes of α and β forms of nylon 6 along the chain axis were determined by Wallner's method. First the shifts of the maximum positions of meridional reflections from their ideal reciprocal‐lattice positions were calculated for the various crystallite sizes. Second, using these relationships, crystallite sizes were estimated from the observed maximum positions of reflections. The estimated values agree well with those from the integral widths of reflections by the method of Hosemann and Wilke.Keywords
This publication has 10 references indexed in Scilit:
- Gitterstörungen in polyäthylenDie Makromolekulare Chemie, 1968
- An infra-red study of the interaction of polyamides with iodine in iodine—potassium iodide solutionPolymer, 1966
- The structure of the gamma form of polycaproamide (Nylon 6)Polymer, 1965
- Crystal structure of the γ‐form of nylon 6Journal of Polymer Science Part A: General Papers, 1965
- Studies on the Crystal Modification of Nylon 6Kobunshi Kagaku, 1963
- Iodine Treatment of Nylon 6Kobunshi Kagaku, 1962
- Studies on the Sorption of Iodine by Polyamide FibersKobunshi Kagaku, 1958
- The crystal structure of polycaproamide: Nylon 6Journal of Polymer Science, 1955
- Über den Einfluß der Kristallitlänge auf die Röntgen-Interferenzen der PolyamideMonatshefte für Chemie / Chemical Monthly, 1948
- Über den Einfluß der Kristallitlänge auf die Röntgen-Interferenzen der PolyamideMonatshefte für Chemie / Chemical Monthly, 1948