Abstract
Pyridine-2-thiolato complexes of copper(I) and cobalt (III) have been prepared from copper(II)- and cobalt(III)-acetylacetonate with pyridine-2-thiol as well as by reacting CuCl(pyridine-2-thiol)3 and CoCl2-(pyridine-2-thiol)2 with a base. The copper(I) complex forms an addition product of low stability with triphenylphosphine. The cobalt complex is monomeric whereas according to its mass spectrum pyridine-2-thiolato-copper(I) appears to be tetrameric.

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