A New Method for the Synthesis of N, N'-Dimethyl Diazacoronands: High-Pressure Alkylation of α, ω-Secondary Diamines with α, ω-Di-Iodo Compounds
- 1 July 1989
- journal article
- research article
- Published by Taylor & Francis in Synthetic Communications
- Vol. 19 (11-12) , 2175-2179
- https://doi.org/10.1080/00397918908052613
Abstract
α, ω-Secondary diamines react under high-pressure conditions with a, α, ω-di-iodo compounds to give the respective diazacoronand dihydroiodides in high yields and their subsequent neutralization followed by distillation affords pure N, N'-dimethyl diazacoronands.Keywords
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