Synthesis and 31P nuclear magnetic resonance studies of trinuclear palladium cluster complexes; X-ray structure of [Pd3Cl(PPh2)2(PEt3)3][BF4]
- 1 January 1977
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 20,p. 709-710
- https://doi.org/10.1039/c39770000709
Abstract
Complexes [Pd3X(PPh2)2(PR3)3][BF4](X = Cl, Br, or SCF3; R = Ph or Et), which are the first examples of trinuclear palladium clusters in an oxidation state other than zero, have been synthesised and characterised by 31P n.m.r. spectroscopy and, in the case of (X = Cl, R = Et)(1), by X-ray diffraction.Keywords
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