FT-IR Analysis of High-Temperature Solid-Phase Reactions Using GC-IR Software
- 1 February 1988
- journal article
- research article
- Published by SAGE Publications in Applied Spectroscopy
- Vol. 42 (2) , 296-298
- https://doi.org/10.1366/0003702884428392
Abstract
A method for following chemical reactions in polymers, using the GC-IR software on an FT-IR spectrometer and a high-temperature thermal cell, is discussed. The method reduces disk access time between the collection of each spectrum, allowing many more data points for kinetic experiments to be collected. The imidization reaction of polyimides above 200°C is given as an example.Keywords
This publication has 12 references indexed in Scilit:
- A reexamination of polyimide formationJournal of Macromolecular Science, Part B, 1986
- Experimental and theoretical study of the effect of medium on chemical imidizationPolymer Science U.S.S.R., 1984
- Kinetics and Mechanism of Thermal Cyclization of Polyamic AcidsPublished by Springer Nature ,1984
- Studies on Thermal Cyclization of Polyamic AcidsPublished by Springer Nature ,1984
- Polyimide Cure DeterminationPublished by Springer Nature ,1984
- Investigation of the kinetics of chemical imidizationPolymer Science U.S.S.R., 1982
- Methods of investigation determining the degree of imidization of polyamidoacidsPolymer Science U.S.S.R., 1979
- Investigations of imidization of polypyromellitamido acids and thermal degradation of polypyromellitimides by mass spectrometric thermal analysisThermochimica Acta, 1979
- Quantitative analysis of imidization and degradation in poly(acid)amide-soluble polyimide systems using the PMR and IR methodsPolymer Science U.S.S.R., 1976
- Studies of thermal cyclizations of polyamic acids and tertiary amine saltsJournal of Polymer Science Part A-1: Polymer Chemistry, 1966