Crystal structure of lead acetate trihydrate
- 1 January 1982
- journal article
- research article
- Published by Walter de Gruyter GmbH in Zeitschrift für Kristallographie
- Vol. 160 (3-4) , 225-233
- https://doi.org/10.1524/zkri.1982.160.3-4.225
Abstract
Lead acetate trihydrate crystallizes in a tetramolecular, monoclinic unit cell of dimensions a = 15.85(1), b = 7.30(1), c = 9.10(1) Å, β = 109.8(5)° in the space group C 2/ m . The crystal structure has been solved by the heavy-atom method and refined to an R value of 0.096 for 790 observed reflections. Nine oxygen atoms belonging to the water molecules and acetate groups coordinate the lead atom whose coordination polyhedron is a monocapped square antiprism. The two crystallographically different acetate groups coordinate both bidentally to the same metal atom. A hydrogen bonding scheme based on the distance criteria has been proposed.Keywords
This publication has 1 reference indexed in Scilit:
- The crystal structure of calcium 5-keto-D-gluconate (calciumD-xylo-5-hexulosonate)Acta Crystallographica, 1965