Combined use of multiple and selective proton-decoupled 13C and 1H n.m.r. spectra for complete proton and carbon-13 resonance assignments of polypeptides
- 1 January 1981
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 5,p. 230-232
- https://doi.org/10.1039/c39810000230
Abstract
Selective proton irradiations during proton and carbon-13 n.m.r. observation demonstrate unequivocal assignments of 1H and 13C resonances of the model peptide valinomycin and the usefulness of this technique in peptide sequencing is noted.Keywords
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