Practical, Large-Scale Synthesis of 2,2-Dimethyl-5-hydroxy-4-oxo-benzo-1,4-dioxin
- 1 April 1994
- journal article
- research article
- Published by Taylor & Francis in Synthetic Communications
- Vol. 24 (7) , 1025-1028
- https://doi.org/10.1080/00397919408020778
Abstract
Modification of a known procedure employing the interaction of thionyl chloride, acetone, and 2,6-dihydroxybenzoic acid was found, to provide the title compound in multikilogram quantities of acceptable yield and purity.Keywords
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