Comparison of High Performance Liquid Chromatography with 1H Nuclear Magnetic Resonance Spectrometry for the Quantitative Analysis of Pyrrolizidine Alkaloids from Senecio Vulgaris
- 1 March 1986
- journal article
- research article
- Published by Taylor & Francis in Journal of Liquid Chromatography
- Vol. 9 (4) , 745-755
- https://doi.org/10.1080/01483918608076666
Abstract
A high-performance liquid chromatographic method for the analysis of pyrrolizidine alkaloids from Senecio vulgaris has been developed using narceine-HCl as an internal standard. A reversed phase procedure with a methanol/.01 M KH2 PO4 30/70 solvent system is described, and compared with a quantitative 1H Nuclear Magnetic Resonance spectrometric method. Some advantages and limitations are discussed.Keywords
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