The Pyrolysis of Trimethylthallium and Evaluation of D[(CH3)2Tl—CH3]
- 1 May 1973
- journal article
- Published by Canadian Science Publishing in Canadian Journal of Chemistry
- Vol. 51 (9) , 1397-1401
- https://doi.org/10.1139/v73-209
Abstract
The pyrolysis of trimethylthallium has been studied in a mercury free toluene carrier flow system (452–536 °K, total pressure 6.7–39.3 mm, contact time 0.9–5.1 s, 5.4–90.2% decomposition). In a vessel cleaned with boiling concentrated HNO3 and coated by decomposing 0.1 g Tl(CH3)3 no heterogeneous reaction could be detected. The extent of reaction measured by product analysis (CH4, C2H6, C6H5C2H5) assuming three CH3 per Tl(CH3)3 undergoing reaction 1Keywords
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