Improved Preparation of 24-Crown-8
- 1 October 1999
- journal article
- research article
- Published by Taylor & Francis in Synthetic Communications
- Vol. 29 (20) , 3555-3560
- https://doi.org/10.1080/00397919908085989
Abstract
An improved method for the preparation of 24-crown-8 is described. Cyclization at room temperature and purification of the crude product via an acetonitrile complex provides a much higher yield than those reported in the literature.Keywords
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