A new class of diosmium(IV) complexes containing both oxide and carboxylate bridges

Abstract
The reactions of the OsVI complexes OsO2X2(PR3)2(X = Cl or Br) with refluxing carboxylic acids produce a new class of osmium dimers of the type Os2(µ-O)(µ-O2CR)2X4(PR3)2 whose structural details have been confirmed by an X-ray diffraction study of Os2(µ-O2CCH3)2Cl4(PPh3)2.

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