Tributyltin Hydride-Induced Free Radical Deoxygenation of the Cyclic Thionocarbonates of Threo-2,3-Dihydroxy Esters and Ketones
- 1 November 1997
- journal article
- research article
- Published by Taylor & Francis in Synthetic Communications
- Vol. 27 (22) , 3887-3893
- https://doi.org/10.1080/00397919708005912
Abstract
A practical and enantiospecific method for the synthesis of optically pure β-hydroxy esters and ketones is described. The key reaction is free radical deoxygenation of the cyclic thionocarbonates of threo-2,3-dihydroxy esters and ketones with tributyltin hydride.Keywords
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