Skeletal characterisation of high nuclearity osmium carbonyl clusters by extended X-ray absorption fine structure (EXAFS) spectroscopy

Abstract
Non-bonded osmium–osmium distances have been identified from the EXAFS of the Os L(III) edge spectra of Os6(CO)18, [N(PPh3)2]2[Os6(CO)18], and [N(PPh3)2]2[Os10C(CO)24] and can be used to characterise the cluster skeleton.

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