Crystal and molecular structure of aquachlorobis(α-picolinato)iron(III)
- 1 January 1976
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in J. Chem. Soc., Dalton Trans.
- No. 15,p. 1438-1440
- https://doi.org/10.1039/dt9760001438
Abstract
The crystal and molecular structure of the title compound has been determined from single-crystal X-ray data and refined by full-matrix least-squares to R 0.035, The yellow-green prismatic crystal of triclinic space group P has unit cell dimensions: a= 8.426(4), b= 14.772(7), c= 7.479(3)Å. α= 97.91(3), β= 131.23(2), and γ= 91.45(3)°. The structure shows FeIII co-ordinated octahedrally to a single carboxy-oxygen, the nitrogen of each of two picolinates, a chloride, and the oxygen of a water molecule.Keywords
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