Assignment of Anomeric Configuration of D-Ribo-, Arabino-, 2′-Deoxyribo-, and 2′,3′-Dideoxyribonucleosides by Noe Difference Spectroscopy
- 1 January 1989
- journal article
- research article
- Published by Taylor & Francis in Nucleosides, Nucleotides and Nucleic Acids
- Vol. 8 (4) , 587-597
- https://doi.org/10.1080/07328318908054200
Abstract
The anomeric configuration of D-ribo-, D-arabi-no, D-2′-deoxyribo-, and D-2′,3′-dideoxyribonucleosides was assigned unambiguously applying n.O.e. difference spectros-copy. For this purpose 1′-H, signals were saturated and the n.O.e. factors of 4′-H, 3′-H, and 2′-H were measured.This publication has 17 references indexed in Scilit:
- 5-Aza-7-deaza-2'-deoxyguanosine: studies on the glycosylation of weakly nucleophilic imidazo[1,2-a]-s-triazinyl anionsThe Journal of Organic Chemistry, 1987
- Assignment of13C Chemical Shifts of α-D-Ribonucleoside Sugar Carbons by1J(CH) Coupling ConstantsNucleosides, Nucleotides and Nucleic Acids, 1985
- Synthesis of imidazo-fused bridgehead-nitrogen 2′-deoxyribo-C-nucleosides: coupling-elimination reactions of 2,5-anhydro-3,4,6-tri-O-benzoyl-D-allonic acidJournal of the Chemical Society, Perkin Transactions 1, 1985
- 2′‐Desoxytubercidin – Synthese eines 2′‐Desoxyadenosin‐Isosteren durch PhasentrasferglycosylierungEuropean Journal of Organic Chemistry, 1983
- Imidazo[1,2-c]pyrimidine nucleosides. Synthesis of N-bridgehead inosine monophosphate and guanosine monophosphate analogs related to 3-deazapurinesThe Journal of Organic Chemistry, 1975
- Recherehes sur les nucleosides de synthese. III. Sur un nouveau critere de determination de la configuration anomere des nucleosides ribosidiquesJournal of Heterocyclic Chemistry, 1973
- Nmr-spektkoskopischeTetrahedron, 1969
- Optical Rotatory Dispersion of Nucleic Acid Derivatives. VIII. The Conformation of Pyrimidine Nucleosides in Solution*Biochemistry, 1967
- Purine Nucleosides. XI. The Synthesis of 2'-Deoxy-9-α- and -β-D-ribofuranosylpurines and the Correlation of Their Anomeric Structure with Proton Magnetic Resonance Spectra1Journal of the American Chemical Society, 1965
- Synthetic Studies of Potential Antimetabolites. IX. The Anomeric Configuration of TubercidinThe Journal of Organic Chemistry, 1963